Microbiological Techniques [STM 312] CLASS FIVE (STERILIZATION)


 Microbiological Techniques [STM 312] CLASS FIVE

STERILIZATION

          Sterilization is the killing or the total elimination of all forms of microbial life including spores, spores are highly resistant to destruction, the term sterilization therefore is an absolute term and the article must be free from all forms of microbial life.
          Disinfection on the other hand is the killing of many organisms with an aim to reduce the number of contaminating organisms to a level that cannot cause infection, during disinfection, some organisms and bacteria spores may survive but pathogenic should be destroyed.
          Disinfectants are the chemicals that are used for disinfection, but they are used only on inanimate objects. Antiseptic on the other hand are mild form of disinfectant which are used externally on living tissues to kill micro-organisms for example on the surface of the skin or on mucus membrane.
          Sterilization is used for sterilizing instrument that are used for surgical procedures for example, gloves, aprons, syringes, scalpels, etc. sterilization is also used in the microbiology laboratory for microbiological works in the microbiology laboratory such as media preparation, reagent, sterilizing equipment and situation in which a sterile condition is to be maintained.



          METHODS FOR STERILLIZATION INCLUDES THE FOLLOWING:
   1.     The use of physical agent
   2.     The use of chemical agent

   1.     The use of physical agent: it includes; i. Heat ii. Radiation iii. And filtration.
i.                   Heat: Heat is the most effective and rapid method for sterilization, heat acts by coagulating cell protein and interfering with the metabolic reactions in the microbial cell. The two most common method of heat sterilization include;
a.     Sterilization by Moist heat
b.     Sterilization by Dry heat
A.   Sterilization by Moist heat: Moist heat act by denaturing and coagulating the cell protein breaking the DNA strands and resulting in a general loss of functional integrity of the cell membrane.
     Sterilization can take place at either 100oC or above 100oC. The following methods are used at 100oC
i.                   Boiling: Boiling at 100oC is done in a water bathe for 30 minutes, instruments such as rubber goods, syringes, surgical instrument that may be damaged at temperatures above 100oC are usually sterilized using this method, by this method, all bacteria and certain spores are destroyed, this method leads to a destruction of all pathogens.
ii.                 Steaming: steaming is more effective than dry heat at the same temperature; this is because steam has more penetrating power due to heat of condensation. Steaming can be done in a steam sterilizer which works at 100oC under a normal atmospheric pressure without any extra pressure, at temperature higher than 100oC, some culture Medias become damaged, and are therefore sterilized using this method. The steam sterilizer is a metallic vessel which has two perforated diaphragm, water is boiled using electricity or gas, and the steam passes through the perforations. At the roof of the steam sterilizer is a small opening where the steam can escape. Sterilization using steam can be done using two different ways;
i.                   Single exposure to the steam continuously for one and the half hours, all pathogens are destroyed, using this method.
ii.                 Fractional sterilization: this method is also known as tynderlization invented by a scientist known as john tyndal. It is used for materials and culture media that are heat labile materials and culture medium, the material is steamed sterilized for 20 minutes, followed by incubation at 37oC overnight, this procedure is repeated for another 2 consecutive days, the spores are allowed to germinate to vegetative cells during the period of incubation and are destroyed during steam sterilization on the second and the third days.

Sterilization above 100oC
Autoclaving is one of the most common methods of sterilization. In autoclaving, sterilization is achieved by the use of steam under pressure. Temperatures used are higher than 100oC and the temperature of boiling used depends on the surrounding atmospheric pressure. When pressure is increased, the temperature of boiling used depends on the surrounding atmospheric pressure. When pressure is increased, the temperature also increases. The autoclave is closed and made air tight. Water starts to boil and the inside pressure increases. The water boils above 100oC. At 15lbs per square inch of pressure, a temperature of 121oC is obtained. When kept for 15 minutes, spores are killed.
PARTS OF AN AUTOCLAVE
An autoclave is a metallic cylindrical vessel. On the lid are;
i.                   Gauge for indicating the pressure.
ii.                 A safety valve which is set to open at any desired pressure.
iii.              A stop clock to release the pressure.

Inside the autoclave is a perforated diaphragm. Water is placed below the diaphragm and heated from below by electricity, gas or stove. To operate an autoclave, the following steps are to be followed;
a.     Place materials into the autoclave.
b.     Close the lid, leave the stop clock open.
c.      Set the safety valve at the desired pressure.
d.     Turn on the heat. Air is forced out until steam comes out through the tap.
e.      Close the top to allow the pressure inside the autoclave to build up until it reaches the set level. At the set level, the safety valve below open and allow excess steam to escape.
f.       Keep this for 15 minute holding time.
g.     Stop the heating.
h.     Cool the Autoclave below 100oC.
i.       Open the stop clock slowly to allow air to enter the autoclave.
To check for the efficiency of an autoclave, the spores of Bacillus steazothermophilus are used. Spores can withstand 121oC heat up to 12 minutes. Strips of paper containing the spores are placed along with materials to be sterilized after autoclaving, the strips are cultured at 50oC - 60oC and checked to see if spores will germinate. If there is no growth, then the autoclave is functioning properly.
PASTEURIZATION
The art of heating at temperature below 100oC aimed at killing pathogenic organism. Pasteurization was developed by a scientist “Louis Pasteur”. It was used for food that are especially heat sensitive when sterilization temperature may alter the nutritive valve of the food or may result in a change of colour, or flavor of the food. Pasteurization does not sterilize the food as many living organism including spores are not destroyed. There are two (2) methods used in pasteurization namely “HTST” (High Temperature Short Time). In this, heating is done at 72oC for 15 seconds or “LTST” (Long Temperature Short Time) In this, heating is done between 63oC - 66oC for 30 minutes.
B.   DRY HEAT STERILIZATION: Dry heat was the first method of sterilization. The process is a larger process than most heat sterilization. The destruction of micro-organisms through the use of dry heat is a gradual phenomenon. With longer exposure to lethal temperatures, the number of micro-organisms that are destroyed increases. A forced ventilation of hot air can be used to increase the rate at which heat is transferred to the organism, and reduce the temperature and amount of time needed to achieve sterility. At higher temperatures, shorter exposure times are required to kill organisms. The mechanism by which dry heat achieves microbial destruction are;
i.                   Protein denaturalization
ii.                 Oxidative damage
iii.              Toxic effect of an elevated electrolyte in the absence of water.
Temperatures used are 160oC held for at least 1 hour to kill moist resistant spores. The articles remain dry. Dry heat has an advantage that it can be used on powders and other heal stable items that are adversely affected by a steam.

I.                  HOT AIR STERILIZATION: the hot air oven is one of the most common methods used for sterilization in the microbiology laboratory. Glass wares, swab sticks, powder and oily substances are sterilized in the hot air oven. A temperature of 160oC is maintained for 1 – 2 hours and at this temperature and holding time, spores are destroyed. This leads to sterilization.
     The hot air oven is an apparatus with double metallic walls and a door. There is an air space between these walls. The apparatus is heated by electricity or gas at the bottom. On heating, the air at the bottom becomes hot and passes between the two walls from below upward and then passes in the inner chamber through the holes on the top of the apparatus. A thermostat is fitted to maintain a constant temperature at 160oC.

II.               FLAMING: Another method of dry heat sterilization is flaming. Flaming is done loops and straight wires. Leaving the loop in the flame of a Bunsen burner or alcohol lamp until it turns red hot. Ensures that any infectious agent gets inactivated. This method is commonly used for small metals or glow objects but it is not suitable for large objects. During initial flaming, infectious materials has a tendency to be sprayed from the wire surface, therefore it is killed, thereby contaminating nearby surfaces and objects. To prevent this, special heaters have been developed which surrounds the inoculating loop with a heated case, ensuring that such case materials does not further contaminate the area. Sometimes, carbon residues are left on the heated object, of the object heat is not enough. To prevent this, the object can be dipped into ethanol, before briefly touching the Bunsen burner flame. The ethanol ignites and turns off leaving fewer residues.

III.           INCINERATION: This is a waste treatment process that involves the combustion of organic substances contained in waste materials. This method also burns any organism off to ash.
     It is used to sterilize medical and bio-hazardous waste before it is discarded with non-hazardous waste.
     “There are mini furnaces created for the purpose of incineration”.






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